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The study covers a thorough assessment of the overall degradation of diclofenac-Na (DCF) by high-frequency ultrasound, focusing particularly on identification, interpretation, and characterization of the oxidation byproducts and their reaction mechanisms. It was found that sonication of 5 mg L−1 DCF at near neutral pH rendered complete conversion of the compound, 45 % carbon, 30 % chlorine, and 25 %...
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