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Reaction of dithiols with Ni(dppe)Cl 2 gave monomeric or dimeric dithiolato compounds depending on the nature of the dithiol. Toluenedithiol (TDT) and 1,2-benzenedithiol (1,2-BDT) gave Ni(dope) (TDT) (1) and Ni(dppe) (1,2-BDT) (2), respectively, whereas 1,3-benzenedithiol (1,3-BDT) gave [Ni(dppe)Cl] 2 (1,3-BDT) (3). Single crystal X-ray diffraction studies of 2 showed a square planar...
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