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The solubility of 3‐(2‐methoxyphenoxy)‐propane‐1,2‐diol, the well‐known chiral drug guaifenesin 1, in water has been investigated by means of polythermal and isothermal approaches. It was found that the solubilities of racemic and enantiomeric diols rac‐ and (R)‐1 depend strongly on temperature. The ternary phase diagram of the guaifenesin enantiomers in water in the temperature range between 10°C...
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