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Lithium monosilicide (LiSi) was formed at high pressures and high temperatures (1.0-2.5GPa and 500-700 o C) in a piston-cylinder apparatus. This compound was previously shown to have an unusual structure based on 3-fold coordinated silicon atoms arranged into interpenetrating sheets. In the present investigation, lowered synthesis pressures permitted recovery of large (150-200mg) quantities...
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