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A novel dimolybdenum complex [(η3-C3H5)(CO)2Mo(μ-S2CPCy3)Mo(η3-CH2CMeCH2)(CO)2], obtained by reacting the [(CO)2(η3-C3H5)Mo(μ-S2CPCy3)Mo(CO)3]− anion with an excess of ClCH2CMe=CH2, has been characterized by i.r., 31P{1H}, 1H- and 13C-n.m.r. spectroscopy and by elemental analysis. The crystal structure of the complex, determined by X-ray diffraction, shows a definite preference for the central carbon...
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