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[MBr(CO) 5 ] reacts with m-ethynylphenylamine and pyridine-2-carboxaldehyde in refluxing tetrahydrofuran to give, fac-[MBr(CO) 3 (py-2-CHN-C 6 H 4 -m-(CCH))] (M=Mn, 1a; Re, 2a). The same method affords the tetracarbonyl [Mo(CO) 4 {py-2-CHN-C 6 H 4 -m-(CCH)}] (3a) starting from [Mo(CO) 4 (piperidine) 2 ]; and the methallyl complex...
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