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An efficient method has been devised for the synthesis of dihydroisobenzofuran derivatives through the reaction of in situ generated ynones with potentially C‐nucleophilic malonate esters. All the products are capable to be prepared by applying the tandem strategy at room temperature. The reaction was realized through a combination of the pivotal TBAF‐catalyzed conjugate addition and selective O‐nucleophilic...
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