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The electrodeposition of Pd onto Pt(111) from PdCl 2 and PdSO 4 containing solutions was studied by cyclic voltammetry and in situ scanning tunnelling microscopy. Pd deposition starts by forming a pseudomorphic monolayer in both cases. While in the presence of chloride this monolayer is deposited at underpotentials, its formation in chloride-free solution is kinetically hindered to...
The electrochemical deposition of palladium onto Au(111) from chloride-containing solutions was investigated by in-situ STM and cyclic voltammetry. These methods are complementary by yielding structural and thermodynamic information. For [PdCl 4 ] 2- adsorbed on Au(111), a distorted hexagonal structure was imaged, and a phase transition within this adsorbed layer was observed...
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