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An internal conversion electron spectrometry with a silicon detector has been used to measure 193m Ir activity in the presence of 192 Ir. The spectrometer consists of a measurement chamber with a high vacuum pump and a tunable accelerating electric field to eliminate X-ray interferences. This electron spectrometry has also been used in conjunction with a gamma-ray spectrometry to determine a number of internal conversion coefficients for 101 Rh and 153 Gd to assist in the derivation of the decay schemes for these radionuclides.