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Differential X‐ray absorption contrast tomography was performed on model ceramic composite systems to image the 3D spatial distributions of Ga and Nd containing phases. The model material systems were fabricated such that they contained two constituent phases. Ga–doped Ba hollandite (Ba1.33Ga2.66Ti5.34O16), and pyrochlore (Nd2Ti2O7) which are under consideration as nuclear waste immobilization matrices...