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Processes associated with the Pd+D alloy codeposition are examined by cyclic voltammetry. The voltammograms cover the potential range: +0.3 to −1.3 V (measured against an Ag/AgCl/KCl (sat) reference) and indicate that the partial current due to the Pd 2+ ion reduction is diffusion limited at slow scan rates. Except for the significant increase in cathodic currents due to D 2 O reduction...