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Efficient charge–carrier separation and their utilization are the key factors in overcoming sluggish four‐electron reaction kinetics involved in photocatalytic oxygen evolution. Here, a novel study demonstrates the significance of Na2S2O8 as a sacrificial agent in comparison to AgNO3. Resultantly, BiFeO3 (BFO) and titanium doped‐oxygen deficient BiFeO3 (Ti‐BFO‐R) nanostructures achieve ≈64 and 44...