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The large strain uniaxial tensile deformation behavior of nylon 6 plasticized by deuterium oxide is investigated by an in situ stretching device built in a deuterium nuclear magnetic resonance (NMR) probe. The D2O molecules probe the environment of the amorphous regions in nylon 6; they do not exist in a “free” state and remain associated with the amide groups by hydrogen bonding during deformation...